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Resultados filtrados por Publicador: Universidade Federal do Rio Grande do Norte; BR; UFRN; Programa de Pós-Graduação em Ciência e Engenharia de Materiais; Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part

Adição de nanopartículas de Ti em matriz de Fe através da deposição por magnetron sputtering

Ferreira, Narayanna Marques
Fonte: Universidade Federal do Rio Grande do Norte; BR; UFRN; Programa de Pós-Graduação em Ciência e Engenharia de Materiais; Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part Publicador: Universidade Federal do Rio Grande do Norte; BR; UFRN; Programa de Pós-Graduação em Ciência e Engenharia de Materiais; Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part
Tipo: Dissertação Formato: application/pdf
POR
Relevância na Pesquisa
67.36%
Microalloyed steels constitute a specific class of steel with low amount of carbon and microalloying elements such as Vanadium (V), Niobium (Nb) and Titanium (Ti). The development and application of microalloyed steels and steels in general are limited to the handling of powders with particles of submicron or nanometer dimensions. Therefore, this work presents an alternative in order to construction of microalloyed steels utilizing the deposition by magnetron sputtering technique as a microalloying element addiction in which Ti nanoparticles are dispersed in an iron matrix. The advantage of that technique in relation to the conventional metallurgical processes is the possibility of uniformly disperse the microalloying elements in the iron matrix. It was carried out deposition of Ti onto Fe powder in high CH4, H2, Ar plasma atmosphere, with two deposition times. After the deposition, the iron powder with nanoparticles of Ti dispersed distributed, were compacted and sintered at 1120 ° C in resistive furnace. Characterization techniques utilized in the samples of powder before and after deposition of Ti were Granulometry, Scanning Electron Microscopy (SEM), energy-dispersive X-ray spectroscopy (EDX) and X-ray diffraction (DRX). In the case of sintered samples...

Construção de um aparato experimental para monitoramento in situ da deposição de filmes finos de titânio por magnetron sputtering; Construction of an experimental apparatus for in situ monitoring of thin film deposition by magnetron sputtering titanium

Nascimento, Igor Oliveira
Fonte: Universidade Federal do Rio Grande do Norte; BR; UFRN; Programa de Pós-Graduação em Ciência e Engenharia de Materiais; Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part Publicador: Universidade Federal do Rio Grande do Norte; BR; UFRN; Programa de Pós-Graduação em Ciência e Engenharia de Materiais; Processamento de Materiais a partir do Pó; Polímeros e Compósitos; Processamento de Materiais a part
Tipo: Dissertação Formato: application/pdf
POR
Relevância na Pesquisa
67.26%
The technique of surface coating using magnetron sputtering is one of the most widely used in the surface engineering, for its versatility in obtaining different films as well as in the micro / nanometric thickness control. Among the various process parameters, those related to the active species of the plasma are of the most fundamental importance in the mechanism and kinetics of deposition. In order to identify the active species of the plasma, parameters such as gas flow, pressure and density of electric power were varied during titanium coating on glass substrate. By flowing argon gas of 10, 20, 30, 40 and 50 sccm (cubic centimeters per minute) for each gas flow a sequential scan of the electric current of 0.10, 0.20, 0.30, 0.40 , 0.50 A. The maximum value of 0.50 A was chosen based both on literature data and on limitations of the equipment. The monitoring of plasma species present during the deposition was carried out in situ by the technique of optical emission spectroscopy (OES) through the spectrometer Ocean Optics USB2000 Series. For this purpose, an apparatus was developed to adapt the OES inside the plasma reactor to stay positioned closest to the target. The radiations emitted by the species were detected by an optical fiber placed behind the glass substrate and their intensities as a function of wavelength were...